CClinicalTrials.gg
CompletedNCT06735235Updated Dec 16, 2024

Salivary Fluoride Clearance

A Phase 1 interventional study of 0 ppm F and 250 ppm F as MFP in Caries, sponsored by Procter and Gamble. Completed at 1 site in United States. Open to participants aged 18 Years and older, including healthy volunteers. Per ClinicalTrials.gov, last updated 2024-12-16.

Sponsored by Procter and Gamble · Phase 1, Interventional, and Basic science

Phase
Phase 1
Study type
Interventional
Enrollment
27
Allocation
Randomized
Ages
18 Years and older
Sex
All
01

Study summary

This is a single-center, four-treatment, four-period crossover study. Over the course of the study, up to thirty qualified subjects will use four (4) study treatment products, one time each according to the randomization. Subjects will brush with 1.25g of the assigned study product at each visit. Subjects will provide saliva samples at baseline and at 2, 6, 12, and 30 minutes post-treatment. The F- concentrations in each saliva sample will be determined by ion chromatography

02

Conditions studied

  • Caries
03

Who can participate

Ages eligible
18 Years and older
Sexes eligible
All
Accepts healthy volunteers
Yes

Inclusion criteria

  • Be at least 18 years of age;
  • Provide written informed consent prior to study participation and be given a signed copy of the Informed Consent form;
  • Be in good general health as determined by the Investigator/Designee based on a review of their medical history;
  • Have at least 16 natural teeth;
  • Have normal salivary flow (0.3-0.6 ml/min) or deemed acceptable by the Investigator/Designee as determined in a previous screening outside of this protocol;
  • Agree not to participate in any other oral care studies for the duration of this study;
  • Agree not to change their current oral care routine except 1) to refrain from using mouth rinse and 2) to agree to use study washout product as designated (current floss users are permitted to continue to floss during this study); viii. Agree to delay elective dentistry, including dental prophylaxis, until study completion, and to report any non-study dentistry received during the course of the study;
  • Agree to refrain from eating, using breath mints, using medicated lozenges, chewing gum, brushing their teeth or drinking within 2 hours of the visit, other than small sips of water up to 30 minutes prior to the visit;
  • Agree to refrain from drinking tea or mineral water, and/or eating sardines within the 12 hours prior to the study visit; and
  • Agree to return for all scheduled visits and to follow all study procedures.

Exclusion criteria

Exclusion Criteria:

  • Active treatment for gingivitis, periodontitis, or caries;
  • Self-reported pregnancy or nursing;
  • Smoking or tobacco chewing;
  • Sjögren syndrome or any other disease/condition causing severe xerostomia;
  • Kidney disease or renal impairment;
  • Undergoing chemotherapy or irradiation procedures;
  • Fixed orthodontic appliances that may interfere with product use;
  • Inability to undergo any study procedures; or
  • Any condition or disease, as determined by the Investigator/Designee that could be expected to interfere with examination procedures or with the subject's safe completion of the study
04

Study design

Phase
Phase 1
Primary purpose
Basic science
Allocation
Randomized
Intervention model
Crossover assignment
Masking
Double (Participant, Investigator)
Enrollment
27 participants (actual)

Study arms

  • Other
    Period 1

    0 ppm F (placebo, negative control), 250 ppm F as MFP (dose-response control), 1100 ppm F as MFP (reference), 2800 ppm F as MFP (dose-response control)

    Drug: 0 ppm F · Drug: 250 ppm F as MFP · Drug: 1100 ppm as MFP · Drug: 2800 ppm F as MFP

  • Other
    Period 2

    0 ppm F (placebo, negative control), 250 ppm F as MFP (dose-response control), 1100 ppm F as MFP (reference), 2800 ppm F as MFP (dose-response control)

    Drug: 0 ppm F · Drug: 250 ppm F as MFP · Drug: 1100 ppm as MFP · Drug: 2800 ppm F as MFP

  • Other
    Period 3

    0 ppm F (placebo, negative control), 250 ppm F as MFP (dose-response control), 1100 ppm F as MFP (reference), 2800 ppm F as MFP (dose-response control)

    Drug: 0 ppm F · Drug: 250 ppm F as MFP · Drug: 1100 ppm as MFP · Drug: 2800 ppm F as MFP

  • Other
    Period 4

    0 ppm F (placebo, negative control), 250 ppm F as MFP (dose-response control), 1100 ppm F as MFP (reference), 2800 ppm F as MFP (dose-response control)

    Drug: 0 ppm F · Drug: 250 ppm F as MFP · Drug: 1100 ppm as MFP · Drug: 2800 ppm F as MFP

Interventions

  • Drug0 ppm F

    Each subject will be randomly assigned to this treatment during one of the four periods for this crossover study.

  • Drug250 ppm F as MFP

    Each subject will be randomly assigned to this treatment during one of the four periods for this crossover study.

  • Drug1100 ppm as MFP

    Each subject will be randomly assigned to this treatment during one of the four periods for this crossover study.

  • Drug2800 ppm F as MFP

    Each subject will be randomly assigned to this treatment during one of the four periods for this crossover study.

05

What researchers measure

Primary outcomes

  1. area under the curve (AUC)

    The primary endpoint will be AUC of the fluoride levels from 2 to 30 minutes. AUC will be calculated for each subject and treatment combination by integrating a 3 parameter first order decay model curve estimate (y= theta1 \* exp (-theta2.X) + theta3). For any values obtained for a timepoint that are below the detection limit, 0.5 times the detection limit will be used. The following rules will apply if a subject has missing value(s) before the AUC is calculated: * If 2 or more timepoints are missing within a period, then the AUC will be set to missing * If only 2-minute data are missing, then curve will be estimated as above * If 6-minute or 12-minute data are missing, a linear imputation between the adjacent timepoints will be used * If 30-minute data are missing, the 12-minute data will be carried forward.

    Time frame: 2-minutes, 6-minutes, 12-minutes, and 30-minutes

06

Study locations

1 site
  • Oral Health Science Center
    Mason, Ohio 45040, United States
07

References and documents

Individual participant data

Plan to share: No

No publications or documents are linked to this record.

08

Registry details

Key details

Study ID
NCT06735235
Lead sponsor
Procter and Gamble
Responsible party
Sponsor
First posted
Dec 16, 2024
Start date
Jul 14, 2021
Primary completion
Jul 29, 2021
Completion
Jul 29, 2021
Last update
Dec 16, 2024

Oversight

Data monitoring committee
No
FDA-regulated drug
No
FDA-regulated device
No
View the source record on ClinicalTrials.gov ↗

Not currently enrolling

This study is completed, as verified in Dec 2024. You cannot join it, but the record below documents what was studied.

Follow this study

Get an email when the registry record changes — status, dates, results — or when someone posts here.

Sign in to follow

Discussion

Questions and observations about this study, from anyone following it. Not medical advice, and not a channel to the study team — their contact details are on the registry record.

Sign in to join the discussion. Reading takes no account; posting does. You choose a display name, and a pseudonym is the default.

Nothing here yet. If you are running this trial, taking part in it, or weighing whether to, this is the place to say so.

Start the discussion